Making of Silver Nanoparticles
0.0010 M silver nitrate solution 0.0010 M 硝酸銀溶液 |
|
---|---|
0.0020 M sodium borohydride solution 0.0020 M 硼氫化鈉溶液 |
|
Saturated sodium chloride solution 飽和氯化鈉溶液 |
|
Use a measuring cylinder to measure 30 cm3 of 0.0020 M sodium borohydride solution. 用適當的量筒量度30 cm3 的0.0020 M硼氫化 鈉溶液。 |
|
Pour the solution into a 100 cm3 beaker. 將其倒在一個100 cm3的燒杯當中。 |
|
Place the beaker into an ice bath. Cool the solution in the ice bath for about 5 - 10 minutes.
|
|
Use a clean measuring cylinder to measure 10 cm3of 0.0010 M silver nitrate solution and transfer the solution into a burette. 用另一個乾淨的量筒量度10 cm3 的0.0010 M 硝酸銀溶液,然後將其倒在滴定管中。 |
|
Stir the NaBH4 solution in the beaker with a magnetic stirrer bar or a glass rod. 用攪拌用磁石或玻璃棒攪拌硼氫化鈉溶液。 |
|
With the beaker containing NaBH4 solution in the ice bath, add the AgNO3 solution dropwise from the burette to the NaBH4 solution in the beaker with continuous stirring, at a rate of about 1 drop per second, until AgNO3 solution is used up. 把硼氫化鈉溶液留在冰浴中,同時攪拌溶液 及用滴定管慢慢滴加硝酸銀溶液,大約1秒1滴 ,直至所有硝酸銀溶液都加進硼氫化鈉溶液中。 |
|
Stop the stirring as soon as the addition of silver nitrate solution is finished, and remove the stirrer bar or glass rod from the mixture. 在所有硝酸銀溶液全部加進硼氫化鈉溶液中, 立刻停止攪拌,然後將攪拌用磁石或玻璃棒從 燒杯中拿出來。 |
|
Observe the mixture and record the observations. 觀察所得到的溶液及記錄觀察結果。 |
|
Place the beaker containing the nanoparticles and a 100 cm3 beaker containing about 40 cm3 of water side by side. 預備另一個裝有大約40 cm3水的100 cm3燒杯, 將盛有銀納米顆粒的燒杯和盛有水的燒杯排列 在一起。 |
|
Turn on a laser pointer from sideway such that the laser beam goes through both the solutions in the beakers. Record the observations. 在其中一個燒杯的一側開啟激光筆,即令激光 束同時透過兩個燒杯。記錄得到的觀察結果。 |
|
Tranfser about half of the silver nanoparticle solution into another 100 cm3 beaker, add about 10 cm3 of saturated NaCl solution into the beaker. 將大約一半的銀納米顆粒溶液倒入另一個 100 cm3的燒杯中,然後加入大約10 cm3 飽和氯化鈉溶液在這個燒杯中。 |
|
Observe for any changes. 觀察其變化。 |